This communication reports a simple, rapid and convenient means of converting sulfonyl chlorides I to thiolsulfonate esters II using a 1:l mixture of iron pentacarbonyl and boron trifluoride ether-ate in N,N-dimethylacetamide (DMAC) or tetramethylurea (TMU). A typical procedure follows. BFx.(C7H5)7
โฆ LIBER โฆ
Reaction of iron pentacarbonyl with an activated vermiculite surface
โ Scribed by M. V. Tsodikov; Ya. R. Katsobashvili; G. A. Korneeva; Yu. V. Maksimov; R. A. Arents
- Book ID
- 112444417
- Publisher
- Springer
- Year
- 1983
- Tongue
- English
- Weight
- 140 KB
- Volume
- 32
- Category
- Article
- ISSN
- 1573-9171
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