𝔖 Bobbio Scriptorium
✦   LIBER   ✦

The synthesis of 2H, 3H, 13C and 14C labelled Mepirzapine

✍ Scribed by F. Sperling; A. van Rooy; F.M. Kaspersen


Publisher
Elsevier Science
Year
1988
Weight
66 KB
Volume
39
Category
Article
ISSN
0883-2889

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


Synthesis of 3H-, 13C3-, and 14C-labeled
✍ C. Flader Lavey; D. Hesk; D. Koharski; V. Truong; P. McNamara πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons 🌐 French βš– 152 KB

## Abstract The preparation of [^3^H]Sch 727965 from unlabeled compound and tritiated water was base catalyzed. Diethyl [^13^C~3~]malonate was used to prepare [^13^C~3~]Sch 727965 in five steps in 21.8% overall yield. In a similar manner, [^14^C]Sch 727965 was prepared in five steps from diethyl [2

Synthesis of 3H, 14C and 13C6 labelled S
✍ D. Hesk; G. Bignan; J. Lee; J. Yang; K. Voronin; C. Magatti; P. McNamara; D. Koh πŸ“‚ Article πŸ“… 2002 πŸ› John Wiley and Sons 🌐 French βš– 130 KB

## Abstract ^3^H‐Sch 58235 was prepared at a specific activity of 29.1 Ci/mmol by Ir(COD)(Cy~3~P)PyPF~6~ catalysed exchange with tritium gas. ^14^C‐Sch 58235 was prepared in three steps from __p__‐hydroxy[ring‐U‐^14^C]benzaldehyde with an overall radiochemical yield of 21%. ^13^C~6~‐Sch 58235 was s

The synthesis of org 3770 labelled with
✍ Frans M. Kaspersen; Fons A. M. Van Rooij; Eric G. M. Sperling; Joop H. Wieringa πŸ“‚ Article πŸ“… 1989 πŸ› John Wiley and Sons 🌐 French βš– 597 KB

The syntheses of 1,2,3,4,10,1412-hexahydro-2-methylpyrazino[2,l-a]pyrido [2,3-c][2]benzazepine (Org 3770) labelled with 'H (and 'H), "C and I4C are described. Tritiated Org 3770 was prepared either by exchange under alkaline conditions with tritiated water or catalytic reductive dehalogenation of a

Synthesis of 2H, 3H and 14C labelled Sch
✍ D. Hesk; T. Duelfer; S. Hickey; D. Hochman; D. Koharski; P. McNamara; S. Saluja πŸ“‚ Article πŸ“… 1994 πŸ› John Wiley and Sons 🌐 French βš– 376 KB

## Abstract ^2^H and ^3^H labelled Sch 40120 were prepared by Pt catalysed exchange with isotopic water. D7‐Sch 40120 was obtained in two exchanges in 53% yield and ^3^H‐Sch 40120 was prepared by a single exchange at a specific activity of 19.8 Ci/mmole. ^14^C‐Sch 40120 was prepared in 4 steps from