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Chloro­[N,N′-di­methyl-N,N′-bis(2-pyridyl­methyl)­ethane-1,2-di­amine]oxovanadium(IV) perchlorate

✍ Scribed by Egdal, Rune Kirk ;Bond, Andrew D. ;McKenzie, Christine J.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
131 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title vanadium complex, [VClO(C 16 H 22 N 4 )]ClO 4 , of the tetradentate ligand N,N H -dimethyl-N,N H -bis(2-pyridylmethyl)ethane-1,2-diamine was obtained from air oxidation of a mixture of the ligand and VCl 3 in wet methanol.

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μ-Oxo-bis{chloro­[N,N′-di­methyl-N,N′-bi
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Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.088 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.