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[N,N-Di­methyl-N'-(2-pyridyl­methyl­ene)­ethane-1,2-di­amine]­di­thio­cyanato­copper(II)

✍ Scribed by Yue, Guo-Ren ;Xu, Xin-Jian ;Shi, Yu-Zhen ;Feng, Lei

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
332 KB
Volume
61
Category
Article
ISSN
1600-5368

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Chloro­[N,N′-di­methyl-N,N′-bis(2-pyridy
Chloro­[N,N′-di­methyl-N,N′-bis(2-pyridyl­methyl)­ethane-1,2-di­amine]oxovanadium(IV) perchlorate
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The title vanadium complex, [VClO(C 16 H 22 N 4 )]ClO 4 , of the tetradentate ligand N,N H -dimethyl-N,N H -bis(2-pyridylmethyl)ethane-1,2-diamine was obtained from air oxidation of a mixture of the ligand and VCl 3 in wet methanol.

N,N′-Di-2-pyridyl­methyl­enedi­amine
N,N′-Di-2-pyridyl­methyl­enedi­amine
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Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.088 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

[N,N′-Dimethyl-N′′-(2-pyridylmethyl­ene)
[N,N′-Dimethyl-N′′-(2-pyridylmethyl­ene)ethane-1,2-diamine]dithio­cyanato­zinc(II)
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The title compound, [Zn(NCS) 2 (C 10 H 15 N 3 )], is a mononuclear zinc(II) complex. The molecule is isostructural with the analogous copper(II) compound [Yue, Xu, Shi & Feng (2005). Acta Cryst. E61, m693-m694]. The Zn atom exhibits a square pyramidal geometry.

[μ-N,N,N′,N′-Tetrakis(2-pyridyl­methyl)-
[μ-N,N,N′,N′-Tetrakis(2-pyridyl­methyl)-1,2-ethanedi­amine]­bis­[di­chloro­copper(II)]
✍ Yoon, Doo-Cheon ;Oh, Chang-Eon ;Lee, Uk 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 142 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.009 A Ê R factor = 0.057 wR factor = 0.136 Data-to-parameter ratio = 19.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.