The title vanadium complex, [VClO(C 16 H 22 N 4 )]ClO 4 , of the tetradentate ligand N,N H -dimethyl-N,N H -bis(2-pyridylmethyl)ethane-1,2-diamine was obtained from air oxidation of a mixture of the ligand and VCl 3 in wet methanol.
Dichloro[N,N-dimethyl-N'-(pyridin-2-ylmethylidene)ethane-1,2-diamine]zinc(II)
✍ Scribed by Sun, Yu-Xi
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 297 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.007 A Ê R factor = 0.026 wR factor = 0.061 Data-to-parameter ratio = 21.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.042 wR factor = 0.132 Data-to-parameter ratio = 10.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.007 A Ê R factor = 0.050 wR factor = 0.126 Data-to-parameter ratio = 11.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.