Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.042 wR factor = 0.089 Data-to-parameter ratio = 12.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
[μ-N,N,N′,N′-Tetrakis(2-pyridylmethyl)-1,2-ethanediamine]bis[dichlorocopper(II)]
✍ Scribed by Yoon, Doo-Cheon ;Oh, Chang-Eon ;Lee, Uk
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 142 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.009 A Ê R factor = 0.057 wR factor = 0.136 Data-to-parameter ratio = 19.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
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The title vanadium complex, [VClO(C 16 H 22 N 4 )]ClO 4 , of the tetradentate ligand N,N H -dimethyl-N,N H -bis(2-pyridylmethyl)ethane-1,2-diamine was obtained from air oxidation of a mixture of the ligand and VCl 3 in wet methanol.
Single-crystal X-ray study T = 113 K Mean '(C±C) = 0.005 A Ê R factor = 0.056 wR factor = 0.163 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
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Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.032 wR factor = 0.034 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Di-l-chloro-bis[chloro(dipyridophenazinej 2 N,N 0 0 0 )copper(II)]