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μ2-Oxalato-κ2O,O′:κ2O′′,O′′′-bis­[aqua­(1,10-phenanthroline-κ2N,N′)copper(II)] dinitrate dihydrate

✍ Scribed by Zhang, Xiang-Dong ;Zhao, Zhen ;Sun, Jin-Yu ;Ma, Yong-Chao ;Zhu, Miao-Li

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
182 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

l 2 -Oxalato-j 2 O,O 0 0 0 :j 2 O 0 0 00 0 0 ,O 0 0 00 0 00 0 0 -bis[aqua(1,10-phenanthroline-j 2 N,N 0 0 0 )copper(II)] dinitrate dihydrate

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In the title dimeric complex, [Cu~2~(C~2~O~4~)Cl~2~(C~12~H~8~N~2~)~2~], which lies on a crystallographic inversion center, the Cu^II^ ion is in a distorted trigonal–bipyramidal coordination geometry formed by two N atoms from a phen ligand, two O atoms from a bridging oxalate ligand and one Cl atom.

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The title mononuclear complex, [Cu(C 2 H 3 O 3 ) 2 (C 12 H 8 N 2 )]Á-2H 2 O, is isostructural with its zinc(II) analogue. The Cu atom in the complex exists in a distorted octahedral coordination environment, defined by four O atoms and two N atoms. O-HÁ Á ÁO hydrogen bonds andstacking interactions h

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✍ Fu, Yun-Long ;Ren, Jia-Lin ;Ng, Seik Weng 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 232 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.004 A Ê R factor = 0.043 wR factor = 0.125 Data-to-parameter ratio = 14.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.