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Total Synthesis of Brevetoxin A: Part 1: First Generation Strategy and Construction of BCD Ring System

✍ Scribed by K. C. Nicolaou; Mark E. Bunnage; Daniel G. McGarry; Shuhao Shi; Patricia K. Somers; Paul A. Wallace; Xin-Jie Chu; Konstantinos A. Agrios; Janet L. Gunzner; Zhen Yang

Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
470 KB
Volume
5
Category
Article
ISSN
0947-6539

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Total Synthesis of Brevetoxin A: Part 2:
Total Synthesis of Brevetoxin A: Part 2: Second Generation Strategy and Construction of EFGH Model System
✍ K. C. Nicolaou; Paul A. Wallace; Shuhao Shi; Michael A. Ouellette; Mark E. Bunna πŸ“‚ Article πŸ“… 1999 πŸ› John Wiley and Sons 🌐 English βš– 252 KB πŸ‘ 1 views

Our second generation strategy for the total synthesis of brevetoxin A involved dissection of the molecule at the ring F oxocene. Synthetically, the F ring formation was expected to occur through Wittig coupling of requisite polycyclic fragments 2 and 3, followed by a hydroxy dithioketal cyclization