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The synthesis of 14C-uniformly ring labeled 3,3′,5,5′-tetra-tert-butyldiphenoquinone

✍ Scribed by J. F. Heeg; G. S. Born; H. C. White

Publisher
John Wiley and Sons
Year
1971
Tongue
French
Weight
251 KB
Volume
7
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

^14^C‐uniformly ring labeled 3,3′,5,5′‐tetra‐tert‐butyldiphenoquinone was synthesized from 2,6‐di‐tert‐butylphenol. Chemical purity was established by mixed melting point, thin‐layer and gas‐liquid chromatography. Radiochemical purity was determined using auto‐radiography in conjunction with thin‐layer chromatography and liquid scintillation techniques. Structure was confirmed by elemental analysis, ultraviolet‐visible and infrared spectroscopy and nuclear magnetic resonance.

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