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The synthesis and purification of 14C-labeled menthol

✍ Scribed by J. F. Debardeleben; R. W. Jenkins; W. C. Bailey; T. S. Osdene

Publisher: John Wiley and Sons
Year: 1969
Tongue: French
Weight: 163 KB
Volume: 5
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2590050308

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✦ Synopsis

The synthesis of 14C-labeled menthol was accomplished by preparation of 14C-labeled (&) pulegone. Catalytic hydrogenation and chemical reduction converted (&) pulegone to the isomeric menthols possessing 1.10 mCi total activity. Gas chromatographic separation of this material gave the relative abundance of each isomer.

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