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Synthesis of p125I -amphetamine

✍ Scribed by D. Duterte; E. Morier; M. le Poncin-Lafitte; J. R. Rapin; R. Rips

Publisher: John Wiley and Sons
Year: 1983
Tongue: French
Weight: 216 KB
Volume: 20
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580200119

No coin nor oath required. For personal study only.

✦ Synopsis

p-iodo-amphetamine was s y n t h e s i z e d by t h e Sandmeyer r e a c t i o n from i o d i n e and p-NH2-amphetamine, i n which t h e amino a l i p h a t i c group was p r o t e c t e d by a n e a s i l y hydrolysable group : t-butyloxycarbonyl. I o d i n e was o b t a i n e d by o x i d a t i o n of Na 1251 with p e r i o d a t e i n a n a c i d i c medium. The y i e l d was 50 'b; w i t h a s p e c i f i c a c t iv i t y o f 25 mCi/rrunol.

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