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Synthesis of New Tetrazole-Substituted Pyroaminoadipic and Pipecolic Acid Derivatives

✍ Scribed by Fatimazohra Lenda; Farhate Guenoun; Bouchra Tazi; Najib Ben larbi; Hassan Allouchi; Jean Martinez; Frédéric Lamaty

Publisher: John Wiley and Sons
Year: 2005
Tongue: English
Weight: 162 KB
Volume: 2005
Category: Article
ISSN: 1434-193X
DOI: 10.1002/ejoc.200400328

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The synthesis of two enantiopure pipecolic acid esters (VI) and (XIII) is reported. Key steps are the intramolecular addition of allyl silane on an iminium double bond, generated via reaction of chiral β-amino alcohols (I) and (VII), with glyoxal (II).