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Synthesis of high specific activity tritium-labelled dotriacontane

✍ Scribed by T. H. Houseman; S. H. Binns; K. Phillips

Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
198 KB
Volume
14
Category
Article
ISSN
0022-2135

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✦ Synopsis

The tobacco smoke p a r t i c u l a t e phase marker d o t r i a c o n t a n e was l a b e l l e d w i t h tritium a t p o s i t i o n s 15, 16, 1 7 and 18 by t h e c a t a l y t i c r e d u c t i o n of dotriaconta-15, 17-diyne. This was obtained by o x i d a t i v e l y coupling hexadec-1-yne, i n t u r n prepared by r e a c t i o n of monosodium a c e t y l i d e w i t h m y r i s t y l bromide.

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