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Synthesis of carbon-14 disulfide and N,N′-dicyclohexylcarbo-14C-diimide

✍ Scribed by C. W. Perry; W. Burger

Publisher
John Wiley and Sons
Year
1977
Tongue
French
Weight
200 KB
Volume
13
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Methyl‐^14^C iodide of high specific activity was converted to carbon‐14 disulfide in quantitative yield by reaction with phosphorus pentasulfide at 300–325°C. Following literature procedures, N,N′ dicyclohexylcarbo‐^14^C‐diimide was prepared in 54% yield from the carbon‐14 disulfide.

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