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Synthesis of [1-14C]n-heptane

✍ Scribed by G. G. David; D. F. C. Morris; E. L. Short

Publisher
John Wiley and Sons
Year
1981
Tongue
French
Weight
123 KB
Volume
18
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Synthesis of n‐heptane labelled with carbon‐14 in the 1‐position is described. The precedure involves five steps starting with reaction of [^14^C]carbon dioxide with n‐hexyl magnesium bromide and finishing with reduction of [1‐^14^C]n‐heptyl bromide. The purity of the final product was more than 97% and the overall yield was 36%.

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