𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis OF 3-[14C]-(p-chlorophenylthio)-2-aminopropane hydrochloride (C 2998-Go)

✍ Scribed by R. K. Maller; K. Nagarajan; M. D. Nair


Publisher
John Wiley and Sons
Year
1985
Tongue
French
Weight
173 KB
Volume
22
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.


📜 SIMILAR VOLUMES


Synthesis and N-methylation of β-14C-p-c
✍ Elizabeth P. Burrows; Elaine Sanders-Bush; H. Joseph Sekerke; Howard E. Smith 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 French ⚖ 309 KB

## Abstract β‐^14^C‐__p__‐Chloroamphetamine hydrochloride was prepared by condensation of carbonyl‐^14^C‐__p__‐chlorobenzaldehyde with nitroethane followed by lithium aluminum hydride (LAH) reduation of the resulting chloro‐phenylnitropropene. After purfication the overall yield was about 25%. N‐Me

Synthesis of 2–14C-3-amino-1-chloro-5-me
✍ Neil J. Lewis; Jan Hes; Philip Yip; Frederick D. Cazer 📂 Article 📅 1977 🏛 John Wiley and Sons 🌐 French ⚖ 180 KB 👁 1 views

## Abstract A convenient synthesis of the ^14^C‐labelled chloromethyl ketone analog of leucine is reported. Modification of previously published conditions allowed for the facile synthesis of: 2–^14^C‐3‐amino‐1‐chloro‐5‐methylhexan‐2‐one hydrochloride in four steps from 1‐^14^C‐DL‐leucine in 85.7%

Synthesis of [Imidazolidinone-2-14C]Go 1
✍ B. Anjaneyulu; K. Nagarajan 📂 Article 📅 1987 🏛 John Wiley and Sons 🌐 French ⚖ 249 KB

Research Centre, Pharma D i v i s i o n HINDUSTAN CIBA-GEIGY LIFlITEO Goregaon, Bombay 400 063, I n d i a S UMMA RY F o r a d d i t i o n a l pharmacokinetic and metabolism S t u d i e s i n l a b o r a t o r y animals and i n humans, Go 10213 was l a b e l l e d w i t h carbon-I4 l o c a t e d on t

Synthesis of 3,3-(14C)-dimethyl-1-phenyl
✍ G. F. Kolar; Ch. Schweickhardt 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 French ⚖ 286 KB

## Abstract 3,3‐(^14^C)‐Dimethyl‐1‐phenyltriazene was prepared from recrystallized benzenediazonium fluoroborate which was coupled with ^14^C‐dimethylamine in excess aqueous sodium carbonate at 0°. The crude product was extracted with ether and purified by distillation. Redistilled ^14^C‐labelled t

Synthesis of 7-[α-(2-amino-[2-14C]thiazo
✍ R. T. Standridge; J. E. Swigor 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 French ⚖ 289 KB 👁 1 views

## Abstract The title compound 9 was prepared by the route outlined in Scheme I. [^14^C]Thiourea (1) was condensed with ethyl 4‐bromo‐3‐oxo‐2‐methoxyiminoacetate (2), providing ethyl 2‐(2‐amino‐4‐[2‐^14^C]thiazolyl)‐2‐methoxyiminoacetate (3), as the pure Z‐isomer. Saponification gave the amino acid