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Synthesis of 2-bromo-[1-14C]ethanamine hydrobromide

✍ Scribed by Peter H. Bach; James W. Bridges

Publisher
John Wiley and Sons
Year
1982
Tongue
French
Weight
232 KB
Volume
19
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

2‐Bromo‐[1‐^14^C]ethanamine hydrobromide (BEA) was synthesized from [2‐^14^C]ethan‐1‐01‐2‐amine hydrochloride, by reaction with HBr in a specially designed chamber at an elevated temperature. The synthetic product was purified in the reaction chamber by fractional vacuum sublimation to give a yield of up to 90% of BEA having a purity greater than 95%.

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