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Synthesis of [2-13C]phenol (1)

✍ Scribed by Sun-Shine Yuan; Alfred M. Ajami

Publisher
John Wiley and Sons
Year
1983
Tongue
French
Weight
221 KB
Volume
20
Category
Article
ISSN
0022-2135

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✦ Synopsis

13 13 [2-C]cyclohexanone was synthesized through [ Clcyanation of cyclopentanone followed by acetylation, reduction and ring expansion. Treatment with cupric bromide/lithium bromide and dehydrobromination of the resulting labeled 1,6-dibromohexanone in a "one pot" procedure gave [2-13C]phenol.

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