✦ LIBER ✦

Synthesis of 1-decene-2-13C

✍ Scribed by Alan P. Marchand; Riza Kaya

Publisher: John Wiley and Sons
Year: 1984
Tongue: French
Weight: 273 KB
Volume: 21
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580210902

No coin nor oath required. For personal study only.

✦ Synopsis

A four-step synthesis of l-decene-2-13C starting w i t h 1-bramxtane (57% overall yield) is described.

📜 SIMILAR VOLUMES

Synthesis of [2-13C]phenol (1)

✍ Sun-Shine Yuan; Alfred M. Ajami 📂 Article 📅 1983 🏛 John Wiley and Sons 🌐 French ⚖ 221 KB

13 13 [2-C]cyclohexanone was synthesized through [ Clcyanation of cyclopentanone followed by acetylation, reduction and ring expansion. Treatment with cupric bromide/lithium bromide and dehydrobromination of the resulting labeled 1,6-dibromohexanone in a "one pot" procedure gave [2-13C]phenol.

Synthesis of 1-13C-1-indanone and 2-13C-

Synthesis of 1-13C-1-indanone and 2-13C-1,2,3,4-tetrahydroquinoline

✍ R. E. Pickering; M. A. Wysocki; E. J. Eisenbraun 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 French ⚖ 229 KB 👁 1 views

Synthesis of 1,2,3,4-tetrahydronaphthale

Synthesis of 1,2,3,4-tetrahydronaphthalene-1-13C, naphthalene-1-13C, and 1-naphthalenol-1-13C

✍ R. E. Pickering; D. L. Bymaster; E. J. Eisenbraun 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 French ⚖ 233 KB

Synthesis of [1,1′ -13C2]-L-cystine

✍ Kenichi Uchida; Masatsune Kainosho 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 French ⚖ 285 KB

## Abstract An improved synthesis of [1,1′‐^13^C~2~]‐L‐cystine which includes the optical resolution of the labeled N‐acetyl‐S‐benzyl‐DL‐cysteine by __Aspergillus__ acylase into __S__‐benzyl‐L‐cysteine is described.

Synthesis of (1, 2-13C2) 2-phosphoglycol

Synthesis of (1, 2-13C2) 2-phosphoglycolic acid

✍ Edward J. O'Connor; York Tomita; Ann E. McDermott 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 French ⚖ 223 KB

## Abstract The synthesis of (1,2‐ ^13^C~2~) 2‐phosphoglycelic acid, 5, from commercially‐available (1,2‐ ^13^C~2~) bromoacetic acid is described along with some of its solution NMR characteristics.

Synthesis of [1-13C]-para-xylene and [2-

Synthesis of [1-13C]-para-xylene and [2-13C]-para-xylene

✍ Michael Mormann; Dietmar Kuck 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 French ⚖ 111 KB

## Abstract An efficient synthesis of [1‐^13^C]‐__para__‐xylene (**1a**) and [2‐^13^C]‐__para__‐xylene (**1b**) is described. The incorporation of the label has been achieved by cyclocondensation of suitable 1,5‐bis(bromomagnesio)alkanes with either ethyl [1‐^13^C]acetate or ethyl [^13^C]formate wh