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Synthesis of [2-13C, 4-13C]-(2R,3S)-catechin and [2-13C, 4-13C]-(2R,3R)-epicatechin

✍ Scribed by Pradeep K. Sharma; Min He; Leo J. Romanczyk Jr; Hagen Schroeter

Publisher
John Wiley and Sons
Year
2010
Tongue
French
Weight
196 KB
Volume
53
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

The first synthesis of doubly labeled, [2‐^13^C, 4‐^13^C]‐(2__R__,3__S__)‐catechin 15 and [2‐^13^C, 4‐^13^C]‐(2R,3__R__)‐epicatechin 18 starting from labeled 2‐hydroxy‐4, 6‐bis(benzyloxy)acetophenone 3 and labeled 3, 4‐bis(benzyloxy)‐benzaldehyde 7 are described. Copyright © 2010 John Wiley & Sons, Ltd.

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