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Synthesis of [15N3]melamine and [13C3]cyanuric acid

✍ Scribed by Yong Luo; Liya Zhang; Weicheng Yang; Weixia Liu; Weijing Lu; Meihua Li

Book ID: 102368325
Publisher: John Wiley and Sons
Year: 2010
Tongue: French
Weight: 69 KB
Volume: 54
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.1835

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✦ Synopsis

Abstract

This report presents an efficient syntheses of two labelled internal standards [^15^N~3~]melamine and [^13^C~3~]cyanuric acid with the common substrates [^15^N]NH~4~Cl and [^13^C]urea, respectively. Both standards with excellent isotopic and chemical purities were prepared in good yields and could be used as internal standards without further purification. Copyright © 2010 John Wiley & Sons, Ltd.

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