Synthesis of [1,3,6,7-15N, 8-13C] adenine
β Scribed by Maria Chiriac; Damian Axente; Nicolae Palibroda; Constantin T. Craescu
- Publisher
- John Wiley and Sons
- Year
- 1999
- Tongue
- French
- Weight
- 254 KB
- Volume
- 42
- Category
- Article
- ISSN
- 0022-2135
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Nitration of I-phenylethyl acetate with NHJ?O,-trijhoroaceiic anhydride gave a mixture of orthoand para-nitro products, which were separable by chromatography ajier saponijication of the acetate. The ortho-isomer [1-(2-nitrophenyl)eihanoll was converted to the 1-(2-nitropheny~ethyl esters of monomet
Three selectively labeled propynes were prepared either with deuterium or carbon-13 at position 3 and doubly labeled with carbon-13 at positions 1 and 2 by an alkylation reaction from the corresponding labeled or unlabeled monolithio acetylides and dimethylsulfates. Their lithiation with nBuLi gave