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1H and 13C spectral assignment of 1,4,5,6,7,8-hexahydroquinolines and their oxa-analogues 5,6,7,8-tetrahydro-4H-chromenes

✍ Scribed by Margarita Suárez; Dolores Molero; Esperanza Salfran; Nazario Martín; Yamila Verdecia; Roberto Martinez; Estael Ochoa; Livan Alba; Margarita Quinteiro; Carlos Seoane


Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
170 KB
Volume
39
Category
Article
ISSN
0749-1581

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Complete 1H and 13C NMR spectral assignm
✍ Cláudia J. Nascimento; Elizabete R. Cruz; J. Daniel Figueroa-Villar 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 91 KB

Unambiguous 1H and 13C chemical shift assignments of the novel antibiotic 6,7,8,9-tetrahydro-7,7dimethyl-dioxolo [5,4-b]acridin-9-one were made using the FUCOUP pulse sequence. The appropriate phase cycling was calculated using the Compact Cartesian Coordinate Product Operator (C3PO) method. Copyrig