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Complete 1H and 13C NMR spectral assignment of 6,7,8,9-tetrahydro-7,7-dimethyldioxolo[5,4-b]acridin-9-one using FUCOUP

✍ Scribed by Cláudia J. Nascimento; Elizabete R. Cruz; J. Daniel Figueroa-Villar

Publisher: John Wiley and Sons
Year: 1999
Tongue: English
Weight: 91 KB
Volume: 37
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199903)37:3<239::aid-mrc445>3.0.co;2-3

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✦ Synopsis

Unambiguous 1H and 13C chemical shift assignments of the novel antibiotic 6,7,8,9-tetrahydro-7,7dimethyl-dioxolo [5,4-b]acridin-9-one were made using the FUCOUP pulse sequence. The appropriate phase cycling was calculated using the Compact Cartesian Coordinate Product Operator (C3PO) method. Copyright

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