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Synthesis of DL-[2-13C, 15N]aspartic acid

✍ Scribed by Robert L. Baxter; Elaine M. Abbot

Publisher
John Wiley and Sons
Year
1985
Tongue
French
Weight
205 KB
Volume
22
Category
Article
ISSN
0022-2135

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✦ Synopsis

A synthesis of the title compound from /13Clparaformaldehyde and [15N)ammonium chloride V f 8 ethyl 2-(1 ,3-/2-13Cldithianyl) acetate 3a is described. Ethyl/3-13C13-oxopropanoate derived in sl'tu from 3a was converted by a stepwise Strecker procedure to DL-[ 2-13C,15Nlaspartic acid 7a.

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