๐”– Bobbio Scriptorium
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Synthesis of 13C1-pinonaldehyde

โœ Scribed by Christopher W. Dicus; Dan Willenbring; Michael H. Nantz

Publisher
John Wiley and Sons
Year
2005
Tongue
French
Weight
107 KB
Volume
48
Category
Article
ISSN
0022-2135

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โœฆ Synopsis

13 C 1 -pinonaldehyde is prepared in seven steps from cis-pinonic acid. In the key sequence, the introduction of labeled carbon is accomplished by Lieben degradation of a methyl ketone followed by treatment of the resultant carboxylic acid with 13 C-methyl lithium.

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