𝔖 Bobbio Scriptorium
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Total synthesis of (1-13C)-glycerol

✍ Scribed by Jill Barber


Publisher
John Wiley and Sons
Year
1985
Tongue
French
Weight
218 KB
Volume
22
Category
Article
ISSN
0022-2135

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Synthesis of 13C1-pinonaldehyde
✍ Christopher W. Dicus; Dan Willenbring; Michael H. Nantz πŸ“‚ Article πŸ“… 2005 πŸ› John Wiley and Sons 🌐 French βš– 107 KB

13 C 1 -pinonaldehyde is prepared in seven steps from cis-pinonic acid. In the key sequence, the introduction of labeled carbon is accomplished by Lieben degradation of a methyl ketone followed by treatment of the resultant carboxylic acid with 13 C-methyl lithium.