Three selectively labeled propynes were prepared either with deuterium or carbon-13 at position 3 and doubly labeled with carbon-13 at positions 1 and 2 by an alkylation reaction from the corresponding labeled or unlabeled monolithio acetylides and dimethylsulfates. Their lithiation with nBuLi gave
A Highly Efficient Synthesis of [1-13C, 18O]- and [1-13C, 2H2]-Glycerol for the Elucidation of Biosynthetic Pathways.
✍ Scribed by Alexandros P. Siskos; Alison M. Hill
- Publisher
- John Wiley and Sons
- Year
- 2003
- Weight
- 51 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0931-7597
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