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Stereoselective Michael addition of trimethyl aluminium to nitro acrylates: a route to 2-methyl-3-amino propionic acid

✍ Scribed by Uwe Eilitz; Frank Leßmann; Oliver Seidelmann; Volkmar Wendisch

Book ID: 104360035
Publisher: Elsevier Science
Year: 2003
Tongue: English
Weight: 77 KB
Volume: 14
Category: Article
ISSN: 0957-4166
DOI: 10.1016/s0957-4166(03)00575-5

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✦ Synopsis

The copper(I)-catalysed Michael addition of trimethyl aluminium to nitro acrylates yields 2-methyl-3-nitro propionic acid esters on a 200 g scale with enantiomeric excesses up to 92%.

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