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Solvothermal Synthesis, Crystal Structure, and Thermal Stability of Three-Layered Thioantimonate(III) Complexes: [Ni(C3H10N2)3]Sb4S7, [C4H14N2]Sb8S13·H2O, and [C6H18N2]Sb10S16·H2O

✍ Scribed by Meng Zhang; Tian Lu Sheng; Xi He Huang; Rui Biao Fu; Xin Wang; Sheng Min Hu; Sheng Chang Xiang; Xin Tao Wu

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
197 KB
Volume
2007
Category
Article
ISSN
1434-1948

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The novel thioantimonate(III) [Fe(C 4 H 13 N 3 ) 2 ]Sb 6 S 10 • 0.5 H 2 O was synthesised under mild hydrothermal conditions by allowing elemental Fe, Sb, and S to react in a 50% diethylenetriamine (dien) solution. The compound crystallises in the monoclinic space group C2/c with a = 33.789(3), b =