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Solvothermal Synthesis, Crystal Structure, and Thermal Stability of Three-Layered Thioantimonate(III) Complexes: [Ni(C3H10N2)3] Sb4S7, [C4H14N2] Sb8S13×H2O, and [C6H18N2] Sb10S16×H2O.

✍ Scribed by Meng Zhang; Tian Lu Sheng; Xi He Huang; Rui Biao Fu; Xin Wang; Sheng Min Hu; Sheng Chang Xiang; Xin Tao Wu

Publisher
John Wiley and Sons
Year
2007
Weight
23 KB
Volume
38
Category
Article
ISSN
0931-7597

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The novel thioantimonate(III) [Fe(C 4 H 13 N 3 ) 2 ]Sb 6 S 10 • 0.5 H 2 O was synthesised under mild hydrothermal conditions by allowing elemental Fe, Sb, and S to react in a 50% diethylenetriamine (dien) solution. The compound crystallises in the monoclinic space group C2/c with a = 33.789(3), b =