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ChemInform Abstract: Solvothermal Synthesis, Crystal Structure, and Thermoanalytical Investigations of the New Layered Thioantimonate(III) [Fe(C4H13N3)2] Sb6S10×0.5H2O.

✍ Scribed by Ralph Staehler; Christian Naether; Wolfgang Bensch

Publisher
John Wiley and Sons
Year
2010
Weight
39 KB
Volume
32
Category
Article
ISSN
0931-7597

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Solvothermal Synthesis, Crystal Structur
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The novel thioantimonate(III) [Fe(C 4 H 13 N 3 ) 2 ]Sb 6 S 10 • 0.5 H 2 O was synthesised under mild hydrothermal conditions by allowing elemental Fe, Sb, and S to react in a 50% diethylenetriamine (dien) solution. The compound crystallises in the monoclinic space group C2/c with a = 33.789(3), b =

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## Abstract As revealed by single crystal XRD compounds (II) and (VI) crystallize in the triclinic space group P$\bar 1$ with Z = 2, (IV) in the monoclinic space group P2~1~/m with Z = 4, and (V) in the monoclinic space group P2~1~/n with Z = 4.