with K-selectride to afford the desired hydroxy compound 24. Desilylation of 24 with HF ' py gave the hydroxy oxime 25. The C=N bond of 25 was reduced with NaBH,CN providing the desired product 26 together with its C4 epimer.[131 Finally, chromatographically purified 26 was deprotected to the target
โฆ LIBER โฆ
Solid-Phase Synthesis of O-Glycopeptide Sequences
โ Scribed by Prof. Dr. Hans Paulsen; Dipl.-Chem. Gunnar Merz; Dipl.-Chem. Udo Weichert
- Publisher
- John Wiley and Sons
- Year
- 1988
- Tongue
- English
- Weight
- 315 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
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