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Solid-Phase Synthesis of Unprotected N-Glycopeptide Building Blocks for SPOT Synthesis of N-linked Glycopeptides

✍ Scribed by Laurence Jobron; Gerd Hummel

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
163 KB
Volume
39
Category
Article
ISSN
0044-8249

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with K-selectride to afford the desired hydroxy compound 24. Desilylation of 24 with HF ' py gave the hydroxy oxime 25. The C=N bond of 25 was reduced with NaBH,CN providing the desired product 26 together with its C4 epimer.[131 Finally, chromatographically purified 26 was deprotected to the target