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Solid phase synthesis of benzamidine and butylamine-derived hydantoin libraries

โœ Scribed by Sang Woong Kim; Jong Sung Koh; Eun Ju Lee; Seonggu Ro

Book ID
110277990
Publisher
Springer
Year
1998
Tongue
English
Weight
61 KB
Volume
3
Category
Article
ISSN
1381-1991

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Solid phase synthesis of hydantoin libra
Solid phase synthesis of hydantoin library using a novel cyclization and traceless cleavage step
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The variety of N, N-disubstituted hydantoin libraries were constructed using derivatives of amino acids, aromatic aldehydes, and isocyanates. The cyclization step of hydantoin was a novel, fast, and clean reaction and completed within five minutes to I hour with neat diisopropylamine. All library co

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An efficient protocol for the preparation of combinatorial libraries is described. The methodology first deploys solid phase chemistry to synthesize a 96-well array of intermediates linked to resin via a latent reactive functionality such as a benzyl ether, tert-amine or thioether. Cleavage from the