COOH C O O H imidazole thiol 8 was accomplished by condensation of 7 with KSCN.['] Subsequent oxidation with Fe,(SO,),[S1 and ion-exchange chromatography (Dowex 50 W x 4, H+-form) afforded
Redox behaviour and reactions of (PhCH2)3Sb; syntheses and structures of [(PhCH2)3SbMe]I and [(PhCH2)3SbMe]3Sb3I12
β Scribed by H.J. Breunig; K.H. Ebert; R. Kaller; Y. Mourad; A. Atmani; Y. Mugnier
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 618 KB
- Volume
- 483
- Category
- Article
- ISSN
- 0022-328X
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
## Abstract The oriented ingots of isostructural compounds Sn~2~SbS~2~I~3~ and Pb~2~SbS~2~I~3~ were prepared using a modified Bridgman method. The lattice parameters of the prepared orthorhombic compounds have been determined by a Xβray powder diffraction analysis. From the spectral response of the
The reaction of PhCH 2 C(O)NR 2 /P(O)Cl 3 (R β«Χ‘β¬ alkyl) with diethyl or triethyl phosphite afforded E-vinylphosphonates 3 with high geometrical stereoselectivity and acceptable yields. The reaction with hydridophosphorane 8 gave 10, a novel trisphosphoranylphosphine oxide that can be reduced to the