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A New Method for the Synthesis of Heterometallic Complexes: Syntheses and Structures of [(PhCH2CH2NLi)3Sb(thf)]2 and [Sb3(cyN)4(NMe2)2]Li

✍ Scribed by Dr. Andrew J. Edwards; Michael A. Paver; Dr. Paul R. Raithby; Moira-Ann Rennie; Christopher A. Russell; Dr. Dominic S. Wright

Publisher: John Wiley and Sons
Year: 1994
Tongue: English
Weight: 377 KB
Volume: 33
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.199412771

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✦ Synopsis

COOH C O O H imidazole thiol 8 was accomplished by condensation of 7 with KSCN.['] Subsequent oxidation with Fe,(SO,),[S1 and ion-exchange chromatography (Dowex 50 W x 4, H+-form) afforded

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