𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Preparation of 2-chloro-6-(2-furanylmethoxy)-4-trichloromethylpyridine-2,6-14C

✍ Scribed by L. H. McKendry


Publisher
John Wiley and Sons
Year
1985
Tongue
French
Weight
264 KB
Volume
22
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

✦ Synopsis


A 1 6 . 7 m C i sample of 99+% r a d i o c h e m i c a l l y p u r e 2-chloro-6-(2-f uranylmethoxy ) -4 -t r i c h l o r o m e t h y l p y r idine-2 , 6 -1 4 C w i t h a s p e c i f i c a c t i v i t y of 13.


📜 SIMILAR VOLUMES


Preparation of 2,3,5,6-tetrachloropyridi
✍ L. H. McKendry 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 390 KB

## Abstract An 88.6% yield of 2,3,5,6‐tetrachloropyridine‐2,6‐^14^C (8.99 mCi, 14.5 mCi/mmole) was obtained __via__ chlorination of 2,6‐dichloropyridine‐2,6‐^14^C.

2, 6-dichloropyridine-2, 6-14C
✍ Lennon H. McKendry; W. W. Muelder 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 French ⚖ 252 KB

2, 6-Dichloropyridine-2, 6-14C with a specific activity of 18.79 mCi/mmole was prepared in a 78% yield the reaction of glutarimide-2,6-14C and PC1 . presents a marked improvement over prevjously reported yields y & this process.

Preparation of 2,4-diamino-6-(diallylami
✍ Richard C. Thomas 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 French ⚖ 202 KB

## Abstract 2,4‐Diamino‐6‐(diallylamino)‐__s__‐triazine‐2,4‐^14^C was prepared from K^14^CN in a four step sequence of reactions. The product was obtained in 26% yield at a specific activity of 1.01 mCi per mM. This product was converted to the hypotensive agent, 2,4‐diamino‐6‐(diallylamino)‐__s__‐

Synthesis of 1-(2,6-difluorobenzoyl)-3-(
✍ Martyn G Gillam 📂 Article 📅 1989 🏛 John Wiley and Sons 🌐 French ⚖ 192 KB 👁 1 views

l-(2,6-Difluorobenzoyl)-3-(2-fluoro-4-(2-chloro-4trifluoromethylphenoxy) [ ring-U-14C]phenyl)urea, a potent new acylurea insecticide and acaricide known as flufenoxuron, was labelled with carbon-14 starting from o-dinitro[ring-U-14C]benzene 1. 2-Fl~oronitro[ring-U-~~C]benzene, 2 obtained by fluorina

Synthese de tris-(dimethylamino-2,4,6) t
✍ Nguyen-Hoang-Nam; Henri Hoellinger; Louis Pichat 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 French ⚖ 211 KB

## Abstract L'hexaméthylmélamine (noyau) ^14^C‐2‐4‐6 (HMM ^14^C), un nouvel agent antitumoral, a été synthétisée à partir de l'urée ^14^C en 2 stades. L'urée ^14^C est cyclisée dans l'o‐dichlorobenzène en acide cyanurique ^14^C‐2‐4‐6, purifié par chromatographie sur colonne d'échangeur d'ions Sépha

The synthesis of 2-chlorobiphenyl-1′,2′,
✍ Paul B. Reichardt; Scott E. Schuttner 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 French ⚖ 170 KB 👁 1 views

## Abstract Modification of the traditional. Gomberg reaction conditions provides a simple, economical. route to 2‐chlorobiphenyl‐1′,2′,3′,4′,5′,6′‐^14^__C__~6~ __(I). The reaction of benzene‐U‐__^14^__C__~6~ __with an excess of the diasonium salt from__ 2__‐chloroaniline produces__ ^14^__C‐labelle