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Preparation du phenyl-3 propene-2 OL-1 14C-3 (alcool cinnamique 14C-3)

✍ Scribed by Nguyen-Hoang-Nam; H. Hoellinger; L. Pichat

Publisher
John Wiley and Sons
Year
1975
Tongue
French
Weight
150 KB
Volume
11
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Methyl cinnamate ‐3‐^14^C is reduced smoothly in excellent yield to cinnamyl alcohol ‐3‐^14^C by aluminum hydride. without attack of the double bond. After purification by column chromatography cinnamyl alcohol ‐3‐^14^C is obtained with a radioactive overall yield of 65% based on cinnamic acid ‐3‐^14^C, specific activity = 9 mCi/mM.

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