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Preparation and application of a new modified liquid chromatographic chiral stationary phase based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid

✍ Scribed by Myung H Hyun; Yoon Jae Cho; Jin Ah Kim; Jong Sung Jin

Book ID
108339200
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
509 KB
Volume
984
Category
Article
ISSN
1873-3778

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πŸ“œ SIMILAR VOLUMES

Liquid chromatographic direct resolution
Liquid chromatographic direct resolution of flecainide and its analogs on a chiral stationary phase based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid
✍ Areum Lee; Hee Jung Choi; Myung Ho Hyun πŸ“‚ Article πŸ“… 2009 πŸ› John Wiley and Sons 🌐 English βš– 346 KB πŸ‘ 2 views

## Abstract Flecainide, an antiarrythmic agent, and its analogs were resolved on a high performance liquid chromatographic chiral stationary phase (CSP) based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid with the use of a mobile phase consisting of methanol‐acetonitrile‐trifluoroacetic acid‐t

Preparation and application of a chiral
Preparation and application of a chiral stationary phase based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid without extra free aminopropyl groups on silica surface
✍ Myung Ho Hyun; Yoon Jae Cho πŸ“‚ Article πŸ“… 2005 πŸ› John Wiley and Sons 🌐 English βš– 713 KB

A crown ether-based chiral stationary phase (CSP) without extra aminopropyl groups on the surface of silica gel was newly prepared by bonding (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid to silica gel. The new CSP was applied to the resolution of various racemic alpha-amino acids, amines, and ami