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Liquid chromatographic direct resolution of β-amino acids on a doubly tethered chiral stationary phase containing NH amide linkage based on (+)-(18-crown-6)- 2,3,11,12-tetracarboxylic acid

✍ Scribed by Myung Ho Hyun; Yanci Song; Yoon Jae Cho; Hee Jung Choi


Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
98 KB
Volume
20
Category
Article
ISSN
0899-0042

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Liquid chromatographic direct resolution
✍ Areum Lee; Hee Jung Choi; Myung Ho Hyun 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 346 KB 👁 2 views

## Abstract Flecainide, an antiarrythmic agent, and its analogs were resolved on a high performance liquid chromatographic chiral stationary phase (CSP) based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid with the use of a mobile phase consisting of methanol‐acetonitrile‐trifluoroacetic acid‐t