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Preparation and application of a new doubly tethered chiral stationary phase containing NCH3 amide linkage based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid

✍ Scribed by Myung Ho Hyun; Yoon Jae Cho; Yanci Song; Hee Jung Choi; Bu Sung Kang

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
364 KB
Volume
19
Category
Article
ISSN
0899-0042

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Resolution of β-amino acids on a high pe
Resolution of β-amino acids on a high performance liquid chromatographic doubly tethered chiral stationary phase containing N–CH3 amide linkage based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid
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## Abstract A doubly tethered chiral stationary phase (CSP) containing N–CH~3~ amide linkage based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid was applied to the resolution of various β‐amino acids. The chiral recognition behaviors for the resolution of β‐amino acids on the doubly tethered C

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## Abstract Flecainide, an antiarrythmic agent, and its analogs were resolved on a high performance liquid chromatographic chiral stationary phase (CSP) based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid with the use of a mobile phase consisting of methanol‐acetonitrile‐trifluoroacetic acid‐t