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Pesticides labelled with 14C III. Synthesis of [6-14C]metribuzine

✍ Scribed by Ernö Koltai; Ferenc Kling; György Rutkai


Publisher
John Wiley and Sons
Year
1996
Tongue
French
Weight
178 KB
Volume
38
Category
Article
ISSN
0022-2135

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✦ Synopsis


14C labelled Metribuzine was synthetised in a five step synthesis firom sodium [l-14C]pivalate (trimethyl acetic acid) via o-brom0-[2-~~C]pinacoline (l-bromo-3,3-dimethyl-butan-2-on) and trimethyl [2-14C]pyruvic acid. The total yield was 30% (calculated on sodium pivalate).


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