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New methods for the synthesis of oxy-functionalized 1,2,4-trioxanes and 1,2,4-trioxepanes from unsaturated hydroperoxy acetals

✍ Scribed by Yoshihiro Ushigoe; Araki Masuyama; Masatomo Nojima; Kevin J. McCullough

Book ID: 104258365
Publisher: Elsevier Science
Year: 1997
Tongue: French
Weight: 206 KB
Volume: 38
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(97)10343-4

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✦ Synopsis

Oxy-functionalized 1,2,4-trioxanes or 1,2,4-trioxepanes were produced by either autoxidation of the unsaturated hydroperoxy acetals 1, or the acid-catalyzed cyclization of epoxy hydroperoxides 9 which were readily prepared from 1. By the appropriate choice of cyclization procedure, the structures of the resulting cyclic peroxides could be efficiently controlled.

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