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N-(4-Nitro­benz­yl)isoquinolinium bis­(2-thioxo-1,3-dithiole-4,5-dithiol­ato)nickelate(III)

✍ Scribed by Li, Jianding ;Yao, Li ;Su, Yang ;Tao, Ruojie

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
288 KB
Volume
62
Category
Article
ISSN
1600-5368

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In the title ion-pair compound, (C 12 H 11 FN)[Ni(C 3 S 5 ) 2 ], the Ni III atom is coordinated by four sulfur atoms of the two 2thioxo-1,3-dithiole-4,5-dithiolate ligands in a square-planar geometry. Weak C-HÁ Á ÁS interactions are found, resulting in a three-dimensional supramolecular network.

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In the title complex, (C~7~H~12~NS)[Ni(C~3~S~5~)~2~], the dihedral angle between the thiazole ring of the cation and the plane of the anion is 8.0 (2)°. In the crystal structure, S...S intermolecular interactions between the anions form a distorted honeycomb structure parallel to the (002) plane, wi