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Measurement of 13 C− 15 N Distances in Uniformly 13 C Labeled Biomolecules: J -Decoupled REDOR

✍ Scribed by Jaroniec, C. P.; Tounge, B. A.; Rienstra, C. M.; Herzfeld, J.; Griffin, R. G.

Book ID
126836384
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
46 KB
Volume
121
Category
Article
ISSN
0002-7863

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13C/15N distance determination by CPMAS
13C/15N distance determination by CPMAS NMR in uniformly 13C labeled molecules
✍ Maggy Hologne; Jésus Raya; Jérôme Hirschinger 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 216 KB

The REDOR and CPMAS techniques are applied for measuring 13C-15N dipolar coupling constants in glycine. It is shown that the selective CP or SPECIFIC CP technique removes the coherent evolution of the spin system under homonuclear 13C-13C J couplings. While the large coupling constant (approximately