13C/15N distance determination by CPMAS
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Maggy Hologne; Jésus Raya; Jérôme Hirschinger
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Article
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2006
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John Wiley and Sons
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English
⚖ 216 KB
The REDOR and CPMAS techniques are applied for measuring 13C-15N dipolar coupling constants in glycine. It is shown that the selective CP or SPECIFIC CP technique removes the coherent evolution of the spin system under homonuclear 13C-13C J couplings. While the large coupling constant (approximately