𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Linear-chain bis(μ-O,O′-di­methyl di­thio­phosphato)­lead(II)

✍ Scribed by Ito, Tetsuzo ;Maeda, Yoshinori

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
177 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 296 K Mean '(O±C) = 0.012 A Ê R factor = 0.029 wR factor = 0.028 Data-to-parameter ratio = 13.4

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

Tris(O,O′-di­methyl­di­thio­phosphato)­c
Tris(O,O′-di­methyl­di­thio­phosphato)­chromium(III)
✍ Ito, Tetsuzo 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 181 KB

The title complex molecule, [Cr(C 2 H 6 O 2 PS 2 ) 3 ], has a twofold rotation axis passing through the Cr atom and a P atom. The Cr atom is coordinated by six S atoms in a distorted octahedral arrangement. The CrÐS bond distances are in the range 2.420 (2)±2.441 (5) A Ê , with an average of 2.429 (

Bis(O,O′-di­cyclo­hexyl di­thio­phosphat
Bis(O,O′-di­cyclo­hexyl di­thio­phosphato-κ2S,S′)­platinum(II)
✍ Kuan, Fong Sheen ;Tiekink, Edward R. T. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 188 KB

Single-crystal X-ray study T = 223 K Mean '(C±C) = 0.009 A Ê R factor = 0.034 wR factor = 0.085 Data-to-parameter ratio = 28.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(4-tert-Butyl-2-methyl­thio­semicarb­azi
(4-tert-Butyl-2-methyl­thio­semicarb­azido)(O-methyl­di­thio­phosphato)­palladium(II)
✍ Janča, Michal ;Taraba, Jan ;Příhoda, Jıří 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 227 KB

The title Pd complex, [Pd(C 6 H 14 N 3 S)(CH 3 O 2 PS 2 )], is formed from Pd(acetate) 2 and 5-tert-butylamino-4-methyl-2-sul®do-2thioxo-1,3,4,2! 5 -thiadiazaphospholan-5-onium, (1), in methanol. The Pd atom is coordinated to two different ligands which are generated in situ as a result of methanoly