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Development of a practical solid-phase synthesis approach to 1,3,5-triazepan-2,6-diones

โœ Scribed by Joel Boeglin; Claire Venin; Gilles Guichard

Book ID
116909587
Publisher
Elsevier Science
Year
2012
Tongue
French
Weight
571 KB
Volume
68
Category
Article
ISSN
0040-4020

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โœ Kyung-Ho Park; Linda J Cox ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 56 KB

A traceless synthesis of 1,2,4-triazolidine-3,5-diones has been achieved through cyclo-elimination from solid-phase. This traceless cyclo-elimination release step is induced by catalytic amount of base or by simply refluxing the urea carbamate intermediate.