Crystal-state 3D-structural characterization of novel, Aib-based, turn and helical peptides
✍ Scribed by Marco Crisma; Erika Andreetto; Marta De Zotti; ALessandro Moretto; Cristina Peggion; Fernando Formaggio; Claudio Toniolo
- Publisher
- John Wiley and Sons
- Year
- 2007
- Tongue
- English
- Weight
- 361 KB
- Volume
- 13
- Category
- Article
- ISSN
- 1075-2617
- DOI
- 10.1002/psc.833
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## Abstract Four diastereomeric‐Leu‐Leu‐Aib‐Leu‐Leu‐Aib‐peptides, Boc‐D‐Leu‐L‐Leu‐Aib‐L‐Leu‐L‐Leu‐Aib‐OMe (1), Boc‐L‐Leu‐D‐Leu‐Aib‐L‐Leu‐L‐Leu‐Aib‐OMe (2), Boc‐L‐Leu‐L‐Leu‐Aib‐D‐Leu‐L‐Leu‐Aib‐OMe (3), and Boc‐L‐Leu‐L‐Leu‐Aib‐L‐Leu‐D‐Leu‐Aib‐OMe (4), were synthesized. The crystals of the four hexape
An exploration of the mixed-ligand system under hydrothermal condition, has led to the isolation of a 3-D Single-crystal X-ray analyses reveal that it crystallizes in the triclinic space group P-1, a = 8.807(4) Å, b =11.139(6) Å, c = 11.291(5) Å, α=75.337( 7), β = 73.584(5), γ= 66.795(5)°. The Cu І